Use of oxalic acid after years of storage

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Use of oxalic acid after years of storage

Post by George » Thu Mar 09, 2017 9:59 am

For a project involving standardising sodium hydroxide solution with analar oxalic acid I have had to make up a 0.1 molar solution of oxalic acid. The oxalic acid used has been in storage for several years (more than 5, I believe) and has formed solid clumps.

My results were inaccurate and I was wondering if the old oxalic acid had absorbed water or somehow reacted after this time. It would explain my results.

I know oxalic acid is a primary standard, but is this a plausible explanation?
Thanks in advance.

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